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Beilstein J. Org. Chem. 2017, 13, 1456–1462, doi:10.3762/bjoc.13.143
Graphical Abstract
Scheme 1: Photo-Meerwein reaction leading to amides.
Figure 1: Products detected in the reaction mixtures during attempts to intercept the radical/cationic interm...
Scheme 2: Reaction of o-alkoxycarbonyldiazonium salts with alkenes under Ru-photocatalyzed conditions.
Scheme 3: Proposed mechanism for the reaction of diazonium salt 2h with methyl methacrylate (3a).
Scheme 4: Reaction of 2-aminocarbonyldiazonium salt 2i with styrene (3b).
Figure 2: The meso-flow apparatus assembled in-house. The components are shown on the left, while the operati...
Scheme 5: Reaction of diazonium salts 11 with styrenes 12. The nucleophilic attack to intermediate A is given...
Scheme 6: Proposed mechanism for the formation of benzo[e][1,3]oxazepin-1(5H)-one 14.
Scheme 7: Investigation of the selectivity of the photochemically induced cyclization.
Beilstein J. Org. Chem. 2016, 12, 139–143, doi:10.3762/bjoc.12.15
Scheme 1: Overall strategy.
Scheme 2: Boc-protected aminoalcohols used as inputs in a diastereoselective Ugi reaction.
Beilstein J. Org. Chem. 2014, 10, 209–212, doi:10.3762/bjoc.10.16
Scheme 1: Synthesis of benzyl azides. a) BnBr, K2CO3, acetone or DMF, rt or 60 °C (for 2d); b) 1) MsCl, Et3N,...
Scheme 2: Synthesis of dihydrobenzoxazepinones 10.